TABLE V

Summary of the Diffusion Sample Set. All Vials Were Prepared with ∼760 Torr of Air in the Headspace

Control Group	Defect	Vial	Wire Size (µm)	Effective Defect Diameter (µm)	Fill	No. of Samples
Positive	Laser-Drilled	2R Glass	—	2	Empty	6
			—	2	PBS	6
			—	5	Empty	6
			—	5	PBS	6
			—	10	Empty	6
			—	10	PBS	6
Type	Microwire	2R Glass	15	0.8	Empty	9
		2 mL Plastic	15	0.5	Empty	6
		2R Glass	41	3.2	Empty	9
		2R Glass		3.2	PBS	9
		2 mL Plastic		2.6	Empty	9
		2 mL Plastic		2.6	PBS	9
		2R Glass	64	8.3	Empty	9
		2R Glass		8.3	PBS	9
		2 mL Plastic		7.4	Empty	9
		2 mL Plastic		7.4	PBS	9
		2R Glass	80	12.9	Empty	9
		2R Glass		12.9	PBS	9
		2 mL Plastic		10.2	Empty	9
		2 mL Plastic		10.2	PBS	9
Gross Positive	Stopper Hole Punch	2R Glass	—	1200	Empty	9
Gross Positive	30G needle	2R Glass	—	159	Empty	6
Negative Control	Unmodified	2R Glass and 2 mL Plastic	—	None	Empty	20 ea.
Negative Control	Unmodified	2R Glass and 2 mL Plastic	—	None	PBS	20 ea.