Helium carrier flow rate: | 1.5 mL/min |
Helium make-up flow rate: | 25 mL/min |
Injector: | Splitless, 270 °C |
Column: | SPB-1 SULFUR, 30 m × 0.32 mm ID, 4.0-μm film |
Oven: | 40 °C (5 min) 10 °C/min to 200 °C (0 min) |
FID temperature; air flow rate, hydrogen flow rate: | 300 °C; 450 mL/min; 40 mL/min |