TABLE VIII

500 ng/mL Spiked Sample Stability Results. Sample Stored in Amber Autosampler Vial on the Benchtop

CompoundInitial Concentration
Day 1 Concentration
% Deviation of Initial ValueDay 2 Concentration
% of Initial ValueDay 3 Concentration
% of Initial Value
(ng/mL)(ng/mL)(ng/mL)(ng/mL)
N-Nitrosodimethylamine136.1141.9104.3142.2104.5148.2108.9
N-Nitrosodiethylamine293.1299.6102.2314.0107.1316.7108.1
N-Nitrosomorpholine278.1273.098.2283.6102.0298.7107.4
N-Nitrosopyrrolidine292.5294.8100.8313.5107.2318.4108.9
N-Nitrosopiperidine354.9351.198.9366.4103.2383.9108.2
N-Nitrosodi-n-butylamine381.8373.497.8406.3106.4437.5114.6