Cycle Details
| Ramp Rate Used | Sucrose Cycle | Sucrose Cycle (annealed) | Mannitol (−5 °C cycle) | Mannitol (−40 °C cycle) |
|---|---|---|---|---|
| Cool rate (°C/min) | 0.5 | 0.5 | 0.5 | 0.5 |
| Freeze (°C) | −40 | −40 | −40 | −40 |
| Anneal (°C) | NA | −15 | −15 | −15 |
| Primary drying (°C) | −40 | −40 & −35 | −5 | −40 |
| Primary drying (h) | 83.0 | 31 & 45 | 41.7 | 49.7 |
| Pressure (mTorr) | 50 | 50 | 1000 | 50 |
| Secondary drying (°C) | 20 | 20 | 20 | 20 |
| Secondary Drying (h) | 4.8 | 5 | 4.5 | 4.7 |
| Pressure (mTorr) | 50 | 50 | 50 | 50 |