TABLE II

Test Product Groups

Group ID	Fill Volume (mL)	Product	Vials in Experiment 1	Vials in Experiment 2	Vials in Experiment 3
1	5 mL	Water	100	100	66
2	10 mL	10% Protein Suspension ∼150 kDa	53	53	35
3	30 mL	10% Protein Suspension ∼150 kDa	50	N/A	N/A
4	50 mL	10% Protein Suspension ∼150 kDa	50	50	N/A
5	100 mL	10% Protein Suspension ∼150 kDa	50	50	38
6	200 mL	10% Protein Suspension ∼150 kDa	50	50	30
7	50 mL	20% Protein Suspension ∼65 kDa	50	50	44
8	100 mL	25% Protein Suspension ∼65 kDa	55	N/A	N/A
9	250 mL	5% Protein Suspension ∼65 kDa	45	45	24
10	500 mL	5% Protein Suspension ∼65 kDa	45	45	12
11	2.2 mL	2500IU Protein Suspension ∼150 kDa	22	N/A	N/A
12	10 mL	Water	100	100	N/A
13	10 mL	Water	40	20	N/A
14	10 mL	Water	100	100	80
15	25 mL	Water	39	N/A	N/A
16	4.4 mL	5000IU Protein Suspension ∼150 kDa	56	N/A	N/A
17	13 mL	15000IU Protein Suspension ∼150 kDa	32	N/A	N/A
18	20 mL	525IU Protein Suspension ∼75 kDa	100	100	100
19	50 mL	925IU Protein Suspension ∼75 kDa	40	20	4
20	4 mL	3000KIU Protein Suspension ∼6.5 kDa	84	N/A	N/A
21	5 mL	3000KIU Protein Suspension ∼6.5 kDa	100	100	26
22	5 mL	Water	100	100	26

Cells marked as N/A did not have any samples available for testing within identified Experiment.