TABLE IV

¹H and ¹³C NMR Assignments for Unknown C

Resonance #	¹H Chemical Shift(^§), ppm^*	Multiplicity^†	Expected # of Protons	¹³C Chemical Shift, ppm^‡
1	1.36	s	54	30.6
2	—	—	—	35.2^§
3	—	—	—	138.2^§
4	6.97	s	6	125.6
5	—	—	—	132.3^§
6	—	—	—	152.9^§
7	2.76	t	6	31.4
8	2.54	t	6	36.6
9	—	—	—	173.2^§
10	4.01	s	6	63.0
11	—	—	—	43.0^§
12	3.97	s	2	63.0
13	—	—	—	172.6^§
14	2.15	na	2	29.0
15	1.93	na	2	31.8
16	—	—	—	81.3^§
17	6.54	s	2	141.1
18	—	—	—	149.8^§
19	—	—	—	35.5^§
20	1.20	s	18	29.6
21	—	—	—	187.2^§
OH	5.27	s	3	—