Extractable Results for the Dichloromethane and Isopropanol Reflux Extracts of the Polypropylene Bottle
| Retention Time (Min) | Name | CAS Number | Identifier Ions | Quantification Data | DCM Reflux Amount (mg/bottle) | IPA Reflux Amount (mg/bottle) |
|---|---|---|---|---|---|---|
| 7.78 | Ethyl-4-ethoxybenzoate | 23676-09-7 | 195.3 (M+H), 167.1 ([M+H]-C2H2) | UV 220 nm | 0.165 | 0.153 |
| 9.06 | 7,9-di-tert-butyl-1-oxaspiro(4,5)deca-6,9-diene-2,8-dione | 82304-66-3 | 231.3 ([M-H]-CO2), 247.3 ([M-H]-CO), 275.3 (M-H) | UV 220 nm | 0.426 | 0.046 |
| 11.59 | Irganox 1010 Degradant 2 | NA | 655.5 (M-H) | UV 220 nm | 0.009 | 0.026 |
| 12.83 | Irganox 1010 Degradant 1 | NA | 915.9 (M-H) | UV 220 nm | 0.236 | 0.189 |
| 13.00 | Irganox 3114 | 27676-62-6 | 564.6 (M-H after side group loss), 219.4 (M+H of side group) | UV 220 nm | 1.24 | 0.334 |
| 14.22 | Irganox 1010 | 6683-19-8 | 1176.3 (M-H) | UV 220 nm | 6.33 | 2.77 |
| 15.06 | Oxidized Irgafos 168 | 95906-11-9 | 663.8 (M+H) | UV 220 nm | 1.84 | 1.17 |
| 15.52 | N,N-ethylene bis(palmitamide) | NA | 535.9 (M-H), 537.8 (M+H) 568.9 (M+O2-), 581.7 (M+NO2-) | APCI− | 0.421 | 0.303 |
| 16.42 | N,N-ethylene bis(palmitamide/stearamide) | NA | 563.9 (M-H), 565.9 (M+H), 596.7 (M+O2-), 609.9 (M+NO2-) | APCI− | 0.474 | 0.149 |
| 16.97 | Irgafos 168 | 31570-04-4 | 473.5 (Hydrolysis Fragment), 647.9 (M+H) | UV 220 nm | 15.9 | 8.00 |