LC Conditions: | |
Solvent gradient: | 0 min: 40/60 methanol/water |
15 min: 100/0 methanol/water | |
30 min: 100/0 methanol/water | |
32 min: 40/60 methanol/water | |
MS parameters: | Atmospheric pressure chemical ionization (APCI) |
Acquisition mode: APCI+/APCI–(Scan) | |
Drying gas temperature: 250 °C | |
Vaporizer temperature: 450 °C | |
Full-scan range: 100–1500 m/z |