CCI Measurements (Helium Leak Rates) of Different Vial Formats Sealed with Bausch & Stroebel or Groninger Capping Equipment
Format | Plunger-Plate Distance (mm) | Pre-Compression Force | Capping Equipment | Turntable Rotation Speed (rpm) | Helium Leak Rate (mbar L/s) |
---|---|---|---|---|---|
6 mL serum | 8.4 | 4.0 bar | Bausch & Stroebel | –183 | 10–8 |
6 mL serum | 8.1 | 4.0 bar | Bausch & Stroebel | –183 | 10–8 |
6 mL serum | 7.7 | 4.0 bar | Bausch & Stroebel | –183 | 10–8 |
6 mL serum | 8.1 | 3.4 bar | Bausch & Stroebel | –183 | 10–8 |
6 mL serum | 8.1 | 5.8 bar | Bausch & Stroebel | –183 | 10–8 |
6 mL serum | 8.1 | 4.0 bar | Bausch & Stroebel | –537 | 10–8 |
6 mL serum | 8.1 | 4.0 bar | Bausch & Stroebel | 145 | 10–8 |
6 mL serum | 8.1 | 4.0 bar | Bausch & Stroebel | 382 | 10–8 |
6 mL serum | 8.1 | 4.0 bar | Bausch & Stroebel | 774 | 10–8 |
15 mL lyo | 8.0 | 4.8 bar | Bausch & Stroebel | –136 | 10–8 |
15 mL lyo | 7.7 | 4.8 bar | Bausch & Stroebel | –136 | 10–8 |
15 mL lyo | 8.0 | 3.2 bar | Bausch & Stroebel | –136 | 10–8 |
15 mL lyo | 8.0 | 4.8 bar | Bausch & Stroebel | –136 | 10–8 |
15 mL lyo | 8.0 | 5.8 bar | Bausch & Stroebel | –136 | 10–8 |
15 mL lyo | 8.0 | 4.8 bar | Bausch & Stroebel | –523 | 10–8 |
15 mL lyo | 8.0 | 4.8 bar | Bausch & Stroebel | +108 | 10–8 |
15 mL lyo | 8.0 | 4.8 bar | Bausch & Stroebel | +352 | 10–8 |
15 mL lyo | 8.0 | 4.8 bar | Bausch & Stroebel | +740 | 10–8 |
6 mL serum | 7.9 | 50 N | Groninger | –145 | 10–8 |
15 mL lyo | 7.9 | 50 N | Groninger | –136 | 10–8 |
20 mL lyo | 7.9 | 50 N | Groninger | +263 | 10–8 |